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Microplastics Solutions

Microplastics

Microplastics solutions for a better life

Microplastics are any solid plastic or synthetic polymer particle insoluble in water with the largest dimension between 1 µm and 5 mm.

Researchers have found microplastics in marine and terrestrial life. It invades the food chain, and it’s even been found in salt, sugar, beer, alcohol, and honey. Not to mention glaciers and rainwater.

Microplastic characterization and identification

Raman spectroscopy plays a key role in identifying the types and origins of microplastics. It’s part of the efforts to develop policies and procedures for controlling the amount of microplastics introduced into our ecosystem. We look at the issues you face, and its effect on the biosphere and human health. 

HORIBA solutions are suitable for beginners as well as for the most demanding users and our expertise and knowledge provide support as you study microplastics.

Characterization of Microplastics video teaser

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        See the complete 26-minute video with the link below. It features an extensive demonstration of HORIBA solutions for micro and nano plastics characterization, including all the steps, from sample preparation to data analysis, using both Raman and AFM techniques.

        What are microplastics

        What are microplastics

        Learn what microplastics are, where it comes from and what risks it poses for our environment and ourselves.
         

        Microplastics analysis

        Microplastics Analysis

        Follow the typical analysis workflow for microplastics separation, counting and identification by means of spectroscopic techniques, and the five key steps required.

        HORIBA solutions

        HORIBA Solutions for Microplastics

        Discover a full solution for scientists by providing all the tools needed for microplastics analysis.
         

        Testimonials

        Watch and read testimonials from scientists working on microplastics.

         

        Application notes & webinars

        Microplastics applications

        Read our application notes and listen to our on-demand webinars to see the results of HORIBA solutions.

        Downloads

        Download the microplastics brochure, microplastics eBook, and other valuable resources.
         

        What are Microplastics

        Microplastics are small bits of plastic, 5 millimeters or less, and either engineered for end-products, or the result of environmental degradation of polymer-based trash.

        Researchers have found microplastics in marine and terrestrial life. It invades the food chain, and it’s even been found in salt, sugar, beer, alcohol, and honey. Not to mention glaciers and rainwater.

        Primary versus secondary microplastics

        What are microplastics?

        What are microplastics?

        Primary microplastics are directly released into the environment as small plastic particles. These are intentionally engineered particles, like those found in some consumer and industrial products. Cosmetics have used microplastics as abrasives.

        Secondary microplastics are the result of the degradation of large plastic waste, like plastic bags and bottles, into smaller plastic fragments when exposed to our environment.

        Why produce microplastics?

        Manufacturers engineer primary microplastics because of the unique physical and chemical properties created by its small scale. Those properties include durability, rigidity and abrasiveness. Density, size, shape and composition influence its properties.

        Scientists use microplastics in many areas, including cosmetics, personal care, detergents, paints/coatings/inks, industrial abrasives, agriculture, pharmaceuticals, wastewater treatment and construction.

        But these particles often weather, degrade or abrade from environmental or physical events, ending up in our oceans and elsewhere.

        Where do primary microplastics come from?

        Ordinary consumer products are the source of most of the ocean’s primary microplastics, according to a study by the International Union for Conservation of Nature (IUCN). That includes synthetic textiles, city dust, tires, road markings, marine coatings, personal care products and engineered plastic pellets.

        What are the health risks of microplastics?

        Microplastics can be toxic, depending on its composition. It can also act as a carrier of other molecules that cling to it. Some of those clinging molecules are bacterial, and others, viral.

        Scientists fear the cumulative buildup of these toxins might affect the health of living organisms. Yet researchers are unsure about the volume of microplastics a body can tolerate or the damage it may cause.

        What we do know is this - consuming microplastics can physically damage organs and leech hazardous chemicals like pesticides. Scientists have shown that these substances can weaken immune function and hinder growth and reproduction.

        The World Health Organization reported in 2019 that the current level of microplastics in drinking water doesn't pose a health risk—yet. But the group said we need to know more.

        Researchers from Johns Hopkins looked at the impact of eating seafood contaminated with microplastics. Their conclusion? The accumulated plastic we take in could damage the immune system and upset a gut's balance.

        Still, the research on health effects are slim. Recent research, through particle analysis and Raman spectroscopy has begun to identify various microplastic types. Scientist are developing sampling, extraction and analysis methods so we can trace these particles back to its sources. That way, we can create public policy to address this potential threat.

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        Microplastics analysis workflow

        Microplastics Analysis

        Microplastics on a plate

        A typical analysis workflow for Microplastics separation, counting and identification by means of spectroscopic techniques requires five main steps: sampling, sample preparation or sample pretreatment, filtration, measurement/data acquisition, and finally, analysis/report.

        1. Sampling
          The Sampling step involves the collection of a matrix and/or different matrices where the Microplastics presence must be investigated.
           
        2. Sample Preparation
          Sample pretreatment is one of the most important steps, since it can influence the accurate identification of the Microplastics during the measurement step. Indeed, the contribution of the matrices (and all the organic contaminants within them) that can interfere with the Microplastics identification must be eliminated.
           
        3. Filtration
          Filters must be carefully selected, considering the wide variety available. Three main characteristics must be considered: Filter size (microplastic concentration, analysis time etc… are driving the choice), filter material (the measurement technique that is tuning this) and pore sizes (which microplastic size we want to analyze).
           
        4. Measure/Data Acquisition
          This is the Chemical/Morphological Identification of the microplastics by the technique of choice. We propose Raman Microscopy, which allows the identification of organic and inorganic particles and assures the analysis of particles from the macro (1 to 5 mm), down to the micron and sub micron ranges.
           
        5. Analysis & Reporting
          Software is a key point for data manipulation and for presenting the results. HORIBA provides fully automated ease-of-use particle analysis software called ParticleFinder, combined with IDFinder, a particle identification software.

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        HORIBA solutions

        The HORIBA bundle

        Considering the Microplastic analysis workflow and the needs and challenges facing scientists approaching it, we developed a full solution to help our existing and future users by providing all the tools needed in a single bundle.

        Our eBook

        • Provides you with an overview of the Microplastics world
        • Explains and details the protocols for sample preparation
        • Summarizes the measurement techniques available and their Pros and Cons
        • Helps you understand Microplastic analysis tips and tricks
        • Keeps you up to date. It will be updated twice a year with new protocols, and other information.

        Filtration kit
        A filtration apparatus to get started with Microplastic analysis.

        Filters, filter holder and VRM (Video Raman Matching)
        A box of Silicon filters with a dedicated holde, developed and optimized for square filters to facilitate the analysis.

        A VRM (Video Raman Matching) stage with patented NanoGPS technology to confidently localize your particles down to the minimum size range allowed.

        Microplastics standard
        A set of tablets with a mixture of polymer particles (PVC, …)  of known size distribution and number to validate your lab environment and workflow.

        Choice of two Raman platforms

        XploRA™ PLUS
        Raman Spectrometer - Confocal Raman Microscope 

         

        LabRAM Soleil
        Raman Microscope

        LabRAM Soleil Raman Microscope full view

        Both Raman microscopes can be equipped with a standard detector (CCD - Charge Couple Device) or imaging detector (EMCCD - Electron Multiplied Charge Couple Device).

        LabSpec 6 is the software platform common to both systems for complete instrument control and data processing, along with additional tools in the Microplastic package. It includes:

        • ParticleFinder™
          ParticleFinder™ offers a user friendly tool for automated location, characterization and Raman analysis of particles. Hundreds or thousands of particles can be quickly located on a video image, analyzed for size and shape descriptors, and then chemically characterized using Raman spectroscopy.
           
        • IDFinder™
          IDFinder™ is an essential tool for managing spectral libraries and automatically identifying thousands of spectra directly in ParticleFinder™ interface. Each spectrum is compared with a dedicated spectral library and a matching coefficient called Hit Quality Index (HQI) is attributed. The component with the highest HQI is recognized as chemical identity of the particle.

        All Microplastics products

        LabRAM Soleil
        LabRAM Soleil

        Raman Spectroscope - Automated Imaging Microscope

        XploRA™ PLUS
        XploRA™ PLUS

        MicroRaman Spectrometer - Confocal Raman Microscope

        LabRAM Odyssey
        LabRAM Odyssey

        Confocal Raman & High-Resolution Spectrometer

        LabRAM Soleil Nano
        LabRAM Soleil Nano

        Real-time and Direct Correlative Nanoscopy

        XploRA Nano
        XploRA Nano

        AFM-Raman for Physical and Chemical imaging

        ParticleFinder
        ParticleFinder

        Automated Particle Measurement, Identification and Classification using Raman Analysis

        IDFinder
        IDFinder

        Spectral Identification Assistant within Raman Spectra Database

        ViewSizer 3000
        ViewSizer 3000

        Simultaneous Multi-Laser Nanoparticle Tracking Analysis (NTA)

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        Testimonials

        Microplastics Researcher Videos

        Microplastics explained part I

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              Dr. Chelsea Rochman breaks down what we know, what we don’t, and what we want to know. Alterra Sanchez describes the big risks and factors involved. 

              Microplastics explained part II

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                  What is Dr. Chelsea Rochman doing with microplastics? Part II gives us a look into the Rochman Lab and the work being done there. Alterra Sanchez tells us the importance of her research as well. 

                  HORIBA solution in action!

                  • Raman XPerience Newsletter - Microplastics pollution
                    Our special issue of HORIBA's Raman XPerience newsletter reviews articles recently published by our customers and highlights the contribution of HORIBA instrumentation to understanding human exposure to microplastic pollution. You can also download the full newsletter here.

                  • Download our application note highlighting microplastics analysis in cosmetics products.
                    Using the example of hand sanitizer, this application note demonstrates how to evaluate whether the product contains synthetic polymer microparticles covered by Microbeads ban.

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                  Applications notes and webinars

                  Microplastics webinars

                  Watch the webinar: Microplastics characterization by Raman microscopy

                  Microplastics characterization by Raman microscopy

                  Microplastics are becoming the 21st century environmental scourge. To control it, more and more regulations are being set in all countries worldwide to monitor the amount of microparticles released in the environment. Thus, some techniques have been identified as reference methods: Pyrolysis GC-MS, Infrared microscopy, and Raman microscopy. This last one provides the best combination of information in both morphological and chemical characterization of each particle down to the micron.
                  During this webinar, we presented how Raman microscopy is becoming the best reference method for microplastics characterization.

                  Microplastics applications

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