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EMGA-930

Oxygen/Nitrogen/Hydrogen Analyzer

This is a simultaneous oxygen, nitrogen & hydrogen elemental analyzer with high accuracy and repeatability suiting to cutting-edge technology's R&D as well as quality control in the market of steel, new materials, catalyst and so on. This is a new generation model optimized to fit to user's requests.

The oxygen is measured as carbon monoxide and carbon dioxide by two non-dispersive infrared detectors, the nitrogen by a thermal conductivity detector and the hydrogen with non dispersive Infra Red detector as H₂O.

Segment: Scientific

Division: Carbon/Sulfur & Oxygen/Nitrogen/Hydrogen Analyzers

Manufacturing Company: HORIBA, Ltd.

Selection of countries and territories where this product is available:
Afghanistan,Albania,Algeria,Andorra,Angola,Antigua and Barbuda,Argentina,Armenia,Australia,Austria,Azerbaijan,Bahamas,Bahrain,Bangladesh,Barbados,Belarus,Belgium,Belize,Benin,Bhutan,Bolivia,Bosnia and Herzegovina,Botswana,Brazil,Brunei,Bulgaria,Burkina Faso,Burundi,Cambodia,Cameroon,Canada,Cape Verde,Cayman Islands,Central African Republic,Chad,Chile,China,Colombia,Comoros,Costa Rica,Cote d'Ivoire,Croatia,Cyprus,Czech,Democratic Republic of the Congo,Denmark,Djibouti,Dominica,Dominican Republic,Ecuador,Egypt,El Salvador,Eritrea,Estonia,Ethiopia,Finland,France,French Guyana,French Polynesia,FYROM (North Macedonia),Gabon,Gambia,Georgia,Germany,Ghana,Greece,Grenada,Guadeloupe,Guatemala,Guinea,Guyana,Haiti,Honduras,Hong Kong SAR of China,Hungary,Iceland,India,Indonesia,Iraq,Ireland,Israel,Italy,Jamaica,Japan,Jordan,Kazakhstan,Kenya,Korea (South),Kosovo,Kuwait,Kyrgiyz Republic,Laos,Latvia,Lebanon,Lesotho,Liberia,Libya,Lichtenstein,Lithuania,Luxembourg,Madagascar,Malawi,Malaysia,Maldives,Mali,Malta,Martinique,Mauritania,Mauritius,Mayotte,Mexico,Moldavia,Monaco,Mongolia,Montenegro,Morocco,Mozambique,Myanmar,Namibia,Nepal,Netherlands,New Caledonia,New Zealand,Nicaragua,Niger,Nigeria,Norway,Oman,Pakistan,Palestine,Panama,Paraguay,Peru,Philippines,Poland,Portugal,Qatar,Republic of the Congo,Reunion,Romania,Russia,Rwanda,Saint Helena,Saint Kitts and Nevis,Sao Tome and Principe,Saudi Arabia,Senegal,Serbia,Seychelles,Sierra Leone,Singapore,Slovakia,Slovenia,Somalia,South Africa,Spain,Sri Lanka,St. Lucia,St. Vincent and the Grenadinas,Sudan,Suriname,Swaziland,Sweden,Switzerland,Taiwan,Tajikistan,Tanzania,Thailand,Togo,Trinidad and Tobago,Tunisia,Turkey,Turkmenistan,Uganda,Ukraine,United Arab Emirates,United Kingdom,Uruguay,Uzbekistan,Venezuela,Vietnam,Yemen,Zambia,Zimbabwe
View the complete list here.

Principle and Gas flow diagram

The sample is placed in a graphite crucible and the crucible is maintained between the upper and the lower electrode of the impulse furnace. A high current power passes through the crucible to create a high temperature.

The oxide in the sample reacts with the graphite crucible, and is extracted as carbon monoxide (CO), and carried together with the carrier gas. The extracted gas is directly analysed after the dust filter. According to the oxygen concentration, it is determined by CO or CO₂ after pass throw oxidizer (Copper Oxide) with a non dispersive Infra-Red analyser (NDIR).

The Hydrogen is determined with a non dispersive Infra Red analyser as H₂O after H₂ passes through the oxidizer (Copper Oxide).

The Nitrogen in the sample is extracted as nitrogen gas (N₂) and its concentration is determined by a thermal conductivity detector (TCD).

Super High Performance

Wide range and high accuracy measurement

*Range: Oxygen:
0-5%, Nitrogen: 0-3%, Hydrogen: 0-0.25%

*Accuracy:
σn-1≦0.3ppm or CV≦1.0% for STD sample
σn-1≦0.02ppm or CV≦0.5% for Reference gas

*Accuracy H:
σn-1≦0.04ppm or RSD≦2.0% for Reference gas

Double detectors of oxygen (CO and CO₂), long type cell and optimized design of TCD provide wide range measurements.

Optimization of the signal processing reduces by half the electrical noise compared to conventional model.

Standard

EMGA fulfils requirements of the standard method for analysis of steel titanium, ceramics etc…

EX)
*ISO10720, ISO17053
*JIS G1228
*ASTM E1019, ASTM E1569, ASTM E1409

User-friendly Software

Measurement Window

Simple software allows easy handling.
Extracted gas signals are displayed in real time numerically and also as curves together with temperature level. Graphs are saved automatically.
In the measurement window, sample weight can be registered automatically. Results are saved in a data table for easy management.

HORIBA originality-Maintenance navigator

Maintenance counter informs users at the timing of consumables replacement to keep high accuracy means.
And as navigator describes the easy to understand procedure for the replacing parts, operator can do maintenance works with absolutely no experience and technical knowledge.

EMGA-930: Oxygen/Nitrogen/Hydrogen analyzer

Principle
Oxygen: Non Dispersive Infrared detector
Nitrogen: Thermal Conductivity detector（TCD）
Hydrogen: Non dispersive Infrared detector (as H₂O)

Measurement range*:
Oxygen: 0-5%, Nitrogen: 0-3%, Hydrogen: 0-0.25%
*Up to 100% wt is possible by decreasing the sample weight.

Sample weight: 1.0 ± 0.1g

Sensitivity(Minimum reading): Oxygen/Nitrogen/Hydrogen: 0.001 ppm.

Accuracy**(Repeatability)
Oxygen/Nitrogen
σn-1≦0.02 ppm or RSD≦0.5% whichever is larger (Reference gas)
σn-1≦0.3 ppm or RSD≦1.0% whichever is larger (Standard sample)
Hydrogen
σn-1≦0.04 ppm or RSD≦2% whichever is larger (Reference gas)
** Based on the sample weight 1.0 ± 0.1g and with automation functions described below

Display
1) Measurement result: LCD or printout
2) Alarm message: LCD or printout
3) Flow sheet: LCD

Power of furnace
Inert gas fusion in impulse furnace
Enable to set the generating power 0 – 8.0 kw

Sample introduction: Dual sample/flux introduction mechanism

Automation functions: Auto cleaner, Crucible loader

Integration conditions:
Preset time integration
Integration up to reach comparator level
Preset time integration or integration up to reach comparator level, whichever is shorter

Sample ID: Enter up to 20 one-byte characters

Calibration

One point or multi point calibration (Reference gas or standard samples)
Calibration using previous analysis data
Calibration curve correction function

Functions

Display of real time extraction curve
Analysis interruption
Self diagnosis and alarm display
Analysis of extraction curve (Superposition, difference etc analysis)
Out put (RC-232C or TCP/IP)

Dimensions: 750mm(H)×785mm(D)×653mm(W)
Sample introduction is positioned at 650mm from table.

Weight: 230kg
On carrying, it is divided in two units (Under 140kg/unit)

Computer: PC model operating OS Windows® XP(SP2) and beyond

Power
Main unit: AC200/220/230/240V ± 10%
Auto cleaner: AC100V (Step-down transformer)
Frequency: 50/60 ± 1Hz

Electric power consumption
Main unit:12kVA (MAX)
Auto cleaner: 1.5kVA (MAX)

Ground resistance: Less than 10Ω

Installation condition
Operation temperature: 5-40°C
Performance temperature: 5-35°C
Humidity: Maximal relative humidity 80％RH between 5-31℃, linearly decrease down to 50％RH between 31-40℃
Vibration: Duplex amplitude 20micron and less than 0.098m/S² accelerations at frequency band

Required gas
He carrier gas: Purity greater than 99.995%, Pressure 0.35MPa
Stainless steel pipe(O.D.3mm) and suitable connecter fitting within 3m of unit
Dry air or N₂ as operating gas: Pressure 0.45MPa
Nylon pipe (O.D.6mm) and suitable connecter fitting within 5m of unit

Cooling mechanism: Radiator unit (Separation type)

Electronic balance (Option)
Enable connection with electronic balance with 1-0.01mg minimum display

Optional automatic voltage regulator (AVR)
Capacity:15kVA
Weight: 130kg

Fully Supported Accessories give simple operation

Purity Analysis in Precious Metal Recycling

While precious metals such as Au, Ag, Pt, and Pd are finite materials, they are essential for electronic components and functional materials. Therefore, it is important to separate and extract the necessary precious metals from the final products and recycle them as high-purity precious metals in order to secure resources and reduce costs. Impurities, which must be controlled, include light elements such as carbon, sulfur, oxygen, and nitrogen. For example, Au (gold) used in electronic devices must be at least 99.999% pure.

Measurement of Oxygen Deficiency in Lithium Manganate

Spinel-type lithium manganate (LiMn2O4-σ) is said to change its discharge characteristics due to slight differences in composition caused by oxygen deficiency. The differences in the discharge characteristics of lithium manganate batteries are also observed in the particle size and crystal structure, but attention is also paid to the difference in the oxygen bonding ratio, as samples with less oxygen bonding have poorer discharge characteristics.

Analysis of Oxygen (O) and Nitrogen (N) in Metal 3D Printer Materials

Stainless steel, Ti, Al, and Cu are commonly used as metal 3D printing materials, and customers have expressed a desire to be able to quickly manage the amounts of oxygen (O) and nitrogen (N) in those materials. For example, if the Ti material contains a large amount of oxygen (O), oxides will be produced, which can lead to defects in the printed part.

EMGA has been designed for accurate measurements of hydrogen content in different sample types such as ferrous metals, non-ferrous metals, semiconductors or electronic materials. The hydrogen content is extracted by fusion of the sample in inert gas and analyzed by a high sensitivity thermal conductivity detector. It is also possible to avoid fusion and extract hydrogen content in the sample by heating below the melting point. The purpose of this note is to explain when to use fusion or solid extraction, the benefits, the applications and samples.

Each year the marketplace sees increasing demands for the analysis of hydrogen contained in various sample materials.

Oxygen and Nitrogen determination in Aluminium Nitride

This application note will show the relevance of the EMGA-920 to measure high level of Nitrogen while maintaining the needed precision for Oxygen determination in AIN.

Oxygen and Nitrogen determination in Boron Nitride

This application note will show the relevance of the EMGA-920 to measure high levels of nitrogen while simultaneously determininig low levels of Oxygen with good precision.

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EMGA-930

Oxygen/Nitrogen/Hydrogen Analyzer

This product is available in the following countries and territories:

Principle and Gas flow diagram

Super High Performance

User-friendly Software

Fully Supported Accessories give simple operation

Request for Information

Inorganic Elemental Analysis

Non-Dispersive Infrared Spectroscopy (NDIR)

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